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dc.contributor.advisorGarzón Ospina, Carlos Mario
dc.creatorVergara Lozano, Giovanny Andrés
dc.date.accessioned2020-07-02T20:32:20Z
dc.date.available2020-07-02T20:32:20Z
dc.date.created2019
dc.identifier.urihttps://repositorio.unal.edu.co/handle/unal/77731
dc.descriptionPor medio de pulverización catódica en atmósfera reactiva se depositaron películas nanoestructuradas, cristalinas y sin nitruros de cromo, sobre sustratos de acero utilizando un blanco del acero austenítico UNS S31603. Estas presentaron estructura ferrítica, austenítica, dúplex (ferrita + austenita) o nitruro MN (M: metal), dependiendo de los parámetros de operación del reactor y del flujo de N2. La concentración de nitrógeno varió desde cero (Ar 1,2 sccm) hasta cerca de 50 %-at (Ar 1,2 sccm + N2 11,2 sccm). La dureza de las películas estuvo entre 8 – 13 GPa, mientras la dureza del blanco fue 2 – 3 GPa. El carácter dúctil – frágil de las películas varió, desde ductilidad muy elevada hasta comportamiento frágil ante cargas de indentación. De forma similar, se obtuvieron películas con elevada adherencia y baja cohesión al sustrato. Este trabajo propone un análisis para explicar la dependencia entre los parámetros de operación del reactor, la estructura, las propiedades mecánicas y las adherencias observadas.
dc.description.abstractStainless Steel (SS) crystalline films, with no chromium nitride formation, were deposited on SS substrates by reactive sputtering, using a UNS S31603 target. Films obtained showed different structures, namely ferrite, austenite, duplex (ferrite + austenite) and MN nitride, according to both operational reactor parameters and N2 flow rate. Nitrogen uptake in film varied between N-lean films (Ar 1,2 sccm) up to near 50 %-at N (Ar 1,2 sccm + N2 11,2 sccm). Films hardness varied 8-13 GPa, while target hardness was around 2 – 3 GPa. Film ductile vs fragile character varied from very high ductile films, up to films with fragile performance films under contact indentation loads. In a similar manner, film-substrate adherence varied from extremely high up to films with cohesive failure, in both micro-indentation and scratch test. In this research, a depth analysis of sputtering parameters, film structure, and film tribomechanical performance is presented.
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dc.format.mimetypeapplication/pdf
dc.language.isospa
dc.rights.urihttp://creativecommons.org/licenses/by-nc-nd/2.5/co/
dc.subjectadherencia
dc.subjectensayo de rayado
dc.subjectnitrógeno en aceros
dc.subjectnitruro MN
dc.subjectpelícula de acero inoxidable
dc.subjectpulverización catódica reactiva
dc.subjectnanodureza
dc.subject.ddc660 - Ingeniería química::669 - Metalurgia
dc.subject.ddc620 - Ingeniería y operaciones afines::629 - Otras ramas de la ingeniería
dc.titleObtención y caracterización de películas nanoestructuradas de austenita expandida depositadas sobre acero inoxidable empleando la técnica de pulverización catódica magnetrón cc en fase reactiva
dc.typeOther
dc.rights.spaAcceso abierto
dc.contributor.institutionUniversidad Nacional de Colombia - Sede Bogotá
dc.subject.keywordadherence
dc.subject.keywordMN nitride
dc.subject.keywordNano hardness
dc.subject.keywordnitrogen in steels
dc.subject.keywordscratch test
dc.subject.keywordstainless steel film
dc.subject.keywordreactive sputtering
dc.type.spaOtro
dc.type.hasversionPublished Version
dc.contributor.gruplacMicroscopía eléctrónica
dc.coverage.modalityMaestria
dc.rights.accessRightsOpen Access
dc.rights.ccAtribución-NoComercial-SinDerivadas 2.5 Colombia
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