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Reducción de la peligrosidad de una escoria de plomo secundario mediante un proceso de vitrificación

dc.rights.licenseAtribución-NoComercial-SinDerivadas 4.0 Internacional
dc.contributor.advisorTorres Agredo, Janneth
dc.contributor.authorNarváez Legarda, Maira Alejandra
dc.date.accessioned2021-09-02T15:40:52Z
dc.date.available2021-09-02T15:40:52Z
dc.date.issued2020
dc.identifier.urihttps://repositorio.unal.edu.co/handle/unal/80080
dc.descriptionIlustraciones, tablas
dc.description.abstractA partir de la problemática de generación y disposición inadecuada de residuos peligrosos, han surgido varios métodos de Estabilización/Solidificación entre los que se encuentra, la vitrificación; este método permite convertir un residuo peligroso en un vitrificado (vidrio), con menor o nula peligrosidad. Una empresa colombiana recupera plomo de baterías usadas de plomo-ácido, mediante fundición secundaria, donde se generan aproximadamente 500 toneladas mensuales de escoria de plomo secundario, residuo catalogado como peligroso por su contenido de metales lixiviables. El objetivo de este estudio fue reducir la peligrosidad de este residuo mediante el proceso de vitrificación, con el fin de facilitar su manejo y/o disposición. Para el desarrollo del estudio, inicialmente se caracterizó el residuo de interés, seguidamente, se llevó a cabo el proceso de vitrificación a nivel laboratorio, donde una mezcla de escoria, arena y carbonato de sodio (Na2CO3), se sometieron a 1000, 1100 y 1200ºC, durante 2 horas. A partir del proceso de vitrificación se encontró que a 1200ºC, se obtuvieron algunos vitrificados homogéneos y mayoritariamente amorfos, sin embargo, en algunas formulaciones se presentaron separaciones cristalinas. Según el análisis ambiental, el proceso de vitrificación fue efectivo, ya que se presentó una reducción significativa en la lixiviación de plomo, cumpliendo con los límites regulados. Además, se obtuvieron valores de dureza Vickers similares a los reportados para vidrios y vidrios cerámicos. Por consiguiente, este estudio aporta a la continuación de investigaciones en Colombia, sobre la aplicación de esta técnica de inertización de residuos peligrosos, especialmente los que se generan en gran cantidad como las escorias de fundición, de tal manera que se logre aprovechar el producto obtenido en diferentes aplicaciones, entre ellas, la industria de la construcción (Texto tomado de la fuente).
dc.description.abstractBeginning with the problem of hazardous waste generation and inappropriate disposal, several methods of Stabilization/Solidification have emerged, among which is, vitrification; this method makes it possible to convert a hazardous waste into a vitrified product (glass), with less or no danger. A Colombian company recovers lead from used lead-acid batteries through secondary smelting, where approximately 500 tons of secondary lead slag are generated per month, which is classified as hazardous due to its leachable metal content. The objective of this study was to reduce the danger of this waste through the vitrification process, in order to facilitate its handling and/or disposal. To perform the study, the residue of interest was initially characterized, then vitrification process was carried out at laboratory scale , where a mixture of slag, sand and sodium carbonate (Na2CO3), were subjected to 1000, 1100 and 1200ºC, for 2 hours. As a result of the vitrification process, it was found that at 1200ºC it was possible to obtain some homogeneous and mostly amorphous vitrification, however in some formulations crystalline separations occurred. According to the environmental analysis, the vitrification process was effective, as there was a significant reduction in lead leaching, complying with the regulated limits. Finally, Vickers hardness values similar to those reported for glass and ceramic glasses were obtained. Consequently, this study contributes to the continuation of research in Colombia on the application of this technique of inertisation of hazardous waste, especially waste generated in large quantities such as foundry slag, in such a way that the product obtained can be used in different applications, including the construction industry.
dc.format.extent79 páginas
dc.format.mimetypeapplication/pdf
dc.language.isospa
dc.publisherUniversidad Nacional de Colombia
dc.rights.urihttp://creativecommons.org/licenses/by-nc-nd/4.0/
dc.subject.ddc620 - Ingeniería y operaciones afines
dc.titleReducción de la peligrosidad de una escoria de plomo secundario mediante un proceso de vitrificación
dc.typeTrabajo de grado - Maestría
dc.type.driverinfo:eu-repo/semantics/masterThesis
dc.type.versioninfo:eu-repo/semantics/publishedVersion
dc.publisher.programPalmira - Ingeniería y Administración - Maestría en Ingeniería - Ingeniería Ambiental
dc.contributor.researchgroupGrupo de Investigación: Materiales y Medio Ambiente (GIMMA)
dc.description.degreelevelMaestría
dc.description.degreenameMagíster en Ingeniería Ambiental
dc.description.methodsA partir de la problemática de generación y disposición inadecuada de residuos peligrosos, han surgido varios métodos de Estabilización/Solidificación entre los que se encuentra, la vitrificación; este método permite convertir un residuo peligroso en un vitrificado (vidrio), con menor o nula peligrosidad. Inicialmente se caracterizó el residuo de interés, seguidamente, se llevó a cabo el proceso de vitrificación a nivel laboratorio, donde una mezcla de escoria, arena y carbonato de sodio (Na2CO3), se sometieron a 1000, 1100 y 1200ºC, durante 2 horas
dc.description.researchareaAprovechamiento de residuos industriales
dc.identifier.instnameUniversidad Nacional de Colombia
dc.identifier.reponameRepositorio Institucional Universidad Nacional de Colombia
dc.identifier.repourlhttps://repositorio.unal.edu.co/
dc.publisher.facultyFacultad de Ingeniería y Administración
dc.publisher.branchUniversidad Nacional de Colombia - Sede Palmira
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dc.rights.accessrightsinfo:eu-repo/semantics/openAccess
dc.subject.proposalEscoria de plomo secundario
dc.subject.proposalEstabilización
dc.subject.proposalSolidificación
dc.subject.proposalVitrificación
dc.subject.proposalResiduos peligrosos
dc.subject.proposalSecondary lead slag
dc.subject.proposalStabilization
dc.subject.proposalSolidification
dc.subject.proposalVitrification
dc.subject.proposalHazardous waste
dc.title.translatedReduction of the hazardousness of a secondary lead slag through a vitrification process
dc.type.coarhttp://purl.org/coar/resource_type/c_bdcc
dc.type.coarversionhttp://purl.org/coar/version/c_970fb48d4fbd8a85
dc.type.contentText
dc.type.redcolhttp://purl.org/redcol/resource_type/TM
oaire.accessrightshttp://purl.org/coar/access_right/c_abf2
oaire.awardtitleEstudio preliminar de inertización de una escoria de plomo secundario a través de un proceso de vitrificación


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