Diseño y evaluación de nanomateriales tipo janus para aplicaciones en procesos de recobro químico mejorado (EOR)
| dc.contributor.advisor | Cortés Correa, Farid Bernardo | spa |
| dc.contributor.advisor | Franco Ariza, Camilo Andrés | spa |
| dc.contributor.author | Giraldo Pedroza, Lady Johana | spa |
| dc.contributor.corporatename | Universidad Nacional de Colombia - Sede Medellín | spa |
| dc.contributor.researchgroup | Fenómenos de Superficie - Michael Polanyi | spa |
| dc.date.accessioned | 2020-03-11T20:55:02Z | spa |
| dc.date.available | 2020-03-11T20:55:02Z | spa |
| dc.date.issued | 2019-04-05 | spa |
| dc.description.abstract | La tecnología de inyección de nanofluidos (nanopartículas dispersas en un fluido de acarreo) ha sido estudiada en reducciones de tensión interfacial, aumentos de viscosidad de fase desplazante y en alteraciones de humectabilidad en la roca; factores que impactan directamente en el número de capilar, favoreciendo aumentos en la recuperación del petróleo. Sin embargo, esta técnica usualmente requiere grandes concentraciones de nanopartículas para ser eficiente en los procesos EOR. Por ello, en este estudio se busca mejorar los nanofluidos con un diseño de nanopartículas novedosas con comportamiento anfifílico, desarrollando nanopartículas Janus con contenido de NiO y surfactante basadas en nanopartículas de SiO2 de dimensión cero (0-D) que pueden ser efectivas en bajas concentraciones. Las nanopartículas sintetizadas fueron caracterizadas por microscopía electrónica de transmisión (TEM), microscopía electrónica de barrido (SEM), análisis DRX, área superficial (SBET), potencial zeta, tensión interfacial (IFT), medidas de reología y alteraciones de humectabilidad y pruebas de desplazamiento. Los resultados mostraron un fuerte aumento del número capilar a concentración muy bajas de nanopartículas Janus, atribuido principalmente a la reducción de IFT en el rango bajo y ultra bajo debido a la alta actividad interfacial de las nanopartículas, conllevando a incrementos en la recuperación de crudo. Las pruebas de desplazamiento presentan un aumento en la eficiencia de hasta un 50% solo con la adición de 100 mg/L de nanopartículas Janus dispersadas en agua, al igual cuando se combinan estas partículas en inyección de surfactantes, donde además de reducir la adsorción del químico (surfactante) en el medio poroso hasta en un 41% también se favorece la disminución de IFT en valores ultrabajo | spa |
| dc.description.abstract | Nanofluid (nanoparticles dispersed in carried fluid) flooding technology has been studied for reduction the interfacial tension, increasing the viscosity of the displacement phase and to alter the rock wettability, which impact directly in capillary number and hence increase the crude oil recovery. However, this technique requires usually large concentration of nanoparticles for being efficient in EOR processes. Therefore, this study aims at improve the nanofluids with a novel design of nanoparticles of amphiphilic behavior, developing NiO and surfactant -containing Janus nanoparticles based on zero-dimension (0-D) SiO2 nanoparticles which can be effective at low concentrations. The nanoparticles synthesized were characterized by Transmission Electron Microscopy (TEM), Scanning Electron Microscopy (SEM), DRX analysis, Surface area (SBET), zeta potential, interfacial tension (IFT), rheology and wettability alteration measurements and coreflooding tests. The results showed a sharply increases of the capillary number at very low concentration of Janus nanoparticles attributed to the decrease of IFT (low and ultra-low values) due to high interfacial activity of nanoparticles, which lead to the increasing of the crude oil recovery. Displacement test present an increase in efficiency up to 50% only with 100 mg/L of Janus nanoparticles dispersed in water, besides when is combined Janus nanoparticles in surfactant flooding too is possible reduce adsorption of the chemical (surfactant) in the porous medium up to 41% and reduce IFT in ultralow values.. | spa |
| dc.description.additional | Magister en Ingeniería de Petróleos | spa |
| dc.description.degreelevel | Maestría | spa |
| dc.format.extent | 102 | spa |
| dc.format.mimetype | application/pdf | spa |
| dc.identifier.uri | https://repositorio.unal.edu.co/handle/unal/76056 | |
| dc.language.iso | spa | spa |
| dc.publisher.branch | Universidad Nacional de Colombia - Sede Medellín | spa |
| dc.publisher.department | Departamento de Procesos y Energía | spa |
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| dc.rights | Derechos reservados - Universidad Nacional de Colombia | spa |
| dc.rights.accessrights | info:eu-repo/semantics/openAccess | spa |
| dc.rights.license | Atribución-NoComercial-SinDerivadas 4.0 Internacional | spa |
| dc.rights.spa | Acceso abierto | spa |
| dc.rights.uri | http://creativecommons.org/licenses/by-nc-nd/4.0/ | spa |
| dc.subject.ddc | 620 - Ingeniería y operaciones afines::622 - Minería y operaciones relacionadas | spa |
| dc.subject.proposal | Nanofluidos | spa |
| dc.subject.proposal | Nanofluids | eng |
| dc.subject.proposal | Janus | spa |
| dc.subject.proposal | Janus | eng |
| dc.subject.proposal | EOR | eng |
| dc.subject.proposal | EOR | spa |
| dc.subject.proposal | Inyección de Agua | spa |
| dc.subject.proposal | Waterflooding | eng |
| dc.subject.proposal | Surfactant flooding | eng |
| dc.subject.proposal | Inyección de surfactantes | spa |
| dc.title | Diseño y evaluación de nanomateriales tipo janus para aplicaciones en procesos de recobro químico mejorado (EOR) | spa |
| dc.type | Trabajo de grado - Maestría | spa |
| dc.type.coar | http://purl.org/coar/resource_type/c_bdcc | spa |
| dc.type.coarversion | http://purl.org/coar/version/c_ab4af688f83e57aa | spa |
| dc.type.content | Text | spa |
| dc.type.driver | info:eu-repo/semantics/masterThesis | spa |
| dc.type.version | info:eu-repo/semantics/acceptedVersion | spa |
| oaire.accessrights | http://purl.org/coar/access_right/c_abf2 | spa |
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