Tratamiento de un agua residual textil contaminada con colorante negro ácido 194 mediante un proceso Electro-Fenton

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dc.contributor.advisorDobrosz-Gómez, Izabela
dc.contributor.advisorQuintero Arias, Jesús David
dc.contributor.authorCastaño Sánchez, Juan Camilo
dc.contributor.cvlacCastaño Sánchez, Juan Camilo [0001887259]spa
dc.contributor.googlescholarCastaño Sánchez, Juan Camilo [9XaaeJwAAAAJ]spa
dc.contributor.orcidCastaño Sánchez, Juan Camilo [000900076418299X]spa
dc.contributor.researchgroupGrupo de Investigación en Procesos Reactivos Intensificados con Separación y Materiales Avanzados (Prisma)spa
dc.date.accessioned2025-04-22T14:02:38Z
dc.date.available2025-04-22T14:02:38Z
dc.date.issued2024
dc.descriptiongraficas, ilustraciones, tablasspa
dc.description.abstractLa industria textil en Colombia ha sido crucial para la economía y la sociedad, aportando cerca del 8% del PIB manufacturero y el 0.9% del PIB nacional. Si bien el papel de esta industria es relevante para la economía, esta genera diferentes tipos de residuos durante el proceso de transformación textil, en donde se destacan los efluentes líquidos generados en la etapa de teñido. Estos efluentes presentan una alta carga contaminante (DQO > 400 mg/L y 41330 unidades Pt-Co), principalmente por la presencia de colorante no fijado a la fibra textil y algunos compuestos asociados a este (cromo y cloruros). El tratamiento y disposición final de este tipo de efluentes sobre cuerpos de agua genera un desafío ambiental (dado que dichos efluentes presentan características tóxicas, carcinógenas, mutagénicas y genotóxicas para diversos organismos) y económico notable. Esta tesis de Maestría en Ingeniería – Ingeniería Química evaluó la capacidad del esquema secuencial coagulación-floculación Electro-Fenton en términos de la degradación de la materia orgánica (cuantificada como DQO y COT) contenida en un agua residual industrial proveniente de la etapa de teñido con el colorante negro ácido 194. A partir de las características fisicoquímicas del efluente coagulado floculado bajo condiciones óptimas se realizó una: (i) identificación de los intervalos de operación para tres procesos Electro-Fenton de celda no dividida; (ii) la selección del proceso Electro-Fenton de mejor desempeño económico y ambiental; y (iii) la optimización de las condiciones de operación mediante la metodología de superficie de respuesta y una optimización multiobjetivo. El proceso Electro-Fenton operado bajo las condiciones óptimas de operación identificadas (j = 8.67 mA/cm2, FH2O2 = 4.89 mg/min, y σ = 5.8 mS/cm) durante un tiempo de 75 minutos permitieron alcanzar una remoción de DQO y COT del 87.0% y 74.2%, respectivamente, con un costo operacional de 4.4 UDSD/m3. De esta forma, la implementación del esquema secuencial coagulación-floculación Electro-Fenton para el tratamiento de un efluente residual industrial contaminado con colorante negro ácido 194 permitió lograr una remoción del 94.9% del DQO, 90.7% del COT, 99.7% de la coloración, disminuir completamente la toxicidad del efluente, a un costo total de operación de 10.4 USD/m3, cumpliendo con los limites estipulados por la normativa ambiental nacional vigente (Texto tomado de la fuente).spa
dc.description.abstractThe textile industry in Colombia has been crucial for the economy and society, contributing around 8% of the manufacturing GDP and 0.9% of the national GDP. While the role of this industry is relevant to the economy, it generates different types of waste during the textile transformation process, with liquid effluents generated during the dyeing stage standing out. These effluents present a high pollutant load (COD > 400 mg/L and 41330 Pt-Co units), mainly due to the presence of dye not fixed to the textile fiber and some compounds associated with it (chromium and chlorides). The treatment and final disposal of this type of effluent into water bodies pose a significant environmental challenge (since these effluents have toxic, carcinogenic, mutagenic, and genotoxic characteristics for various organisms) and a notable economic burden. This Master's thesis in Engineering – Chemical Engineering evaluated the capacity of the sequential coagulation-flocculation Electro-Fenton scheme in terms of the degradation of organic matter (quantified as COD and TOC) contained in an industrial wastewater originating from the dyeing stage using acid black 194 dye. Based on the physicochemical characteristics of the coagulated flocculated effluent under optimal conditions, the following were performed: (i) identification of the operating ranges for three non-divided cell Electro-Fenton processes; (ii) selection of the Electro-Fenton process with the best economic and environmental performance; and (iii) optimization of the operating conditions using response surface methodology and multi-objective optimization. The Electro-Fenton process operated under the identified optimal operating conditions (j = 8.67 mA/cm², FH2O2 = 4.89 mg/min, and σ = 5.8 mS/cm) for 75 minutes achieved COD and TOC removal rates of 87.0% and 74.2%, respectively, with an operational cost of 4.4 USD/m³. Thus, the implementation of the sequential coagulation-flocculation Electro-Fenton scheme for treating industrial wastewater contaminated with acid black 194 dye achieved a 94.9% COD removal, 90.7% TOC removal, 99.7% color removal, eliminated the effluent’s toxicity, and had a total operational cost of 10.4 USD/m³, meeting the limits stipulated by the current national environmental regulations.eng
dc.description.curricularareaQuímica Y Procesos.Sede Manizalesspa
dc.description.degreelevelMaestríaspa
dc.description.degreenameMagíster en Ingeniería - Ingeniería Químicaspa
dc.description.researchareaProcesos Avanzados de Oxidaciónspa
dc.description.researchareaTratamiento de Aguas Residuales Industrialesspa
dc.format.extentxxix, 214 páginasspa
dc.format.mimetypeapplication/pdfspa
dc.identifier.instnameUniversidad Nacional de Colombiaspa
dc.identifier.reponameRepositorio Institucional Universidad Nacional de Colombiaspa
dc.identifier.repourlhttps://repositorio.unal.edu.co/spa
dc.identifier.urihttps://repositorio.unal.edu.co/handle/unal/88032
dc.language.isospaspa
dc.publisherUniversidad Nacional de Colombiaspa
dc.publisher.branchUniversidad Nacional de Colombia - Sede Manizalesspa
dc.publisher.facultyFacultad de Ingeniería y Arquitecturaspa
dc.publisher.placeManizales, Colombiaspa
dc.publisher.programManizales - Ingeniería y Arquitectura - Maestría en Ingeniería - Ingeniería Químicaspa
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dc.relation.referencesSalazar Sogamoso, L. M. (2025). Decoloración y Mineralización de un Agua Residual Industrial Textil mediante un Proceso Electro-Fenton con generación de H2O2 in-situ. (Tesis presentada como requisito parcial para optar al título de: Magíster en Ingeniería – Ingeniería Ambiental). Universidad Nacional de Colombia sede Manizales, Facultad de Ingeniería y Arquitectura.spa
dc.rights.accessrightsinfo:eu-repo/semantics/openAccessspa
dc.rights.licenseAtribución-NoComercial 4.0 Internacionalspa
dc.rights.urihttp://creativecommons.org/licenses/by-nc/4.0/spa
dc.subject.ddc600 - Tecnología (Ciencias aplicadas)::607 - Educación, investigación, temas relacionadosspa
dc.subject.ddc620 - Ingeniería y operaciones afines::629 - Otras ramas de la ingenieríaspa
dc.subject.proposalAgua Residual Industrial Textilspa
dc.subject.proposalColorante Negro Ácido 194spa
dc.subject.proposalProceso Electroquímico Avanzado de Oxidaciónspa
dc.subject.proposalElectro-Fentonspa
dc.subject.proposalPeroxidación electroquímicaspa
dc.subject.proposalPeroxi-Coagulaciónspa
dc.subject.proposalOptimización multiobjetivospa
dc.subject.proposalIndustrial Textile Wastewatereng
dc.subject.proposalAcid Black 194 Dyeeng
dc.subject.proposalAdvanced Electrochemical Oxidation Processeng
dc.subject.proposalElectro-Fentoneng
dc.subject.proposalElectrochemical Peroxidationeng
dc.subject.proposalPeroxi-coagulationeng
dc.subject.proposalMulti-objective Optimizationeng
dc.subject.unescoAgua residualspa
dc.subject.unescoWaste watereng
dc.subject.unescoTratamiento del aguaspa
dc.subject.unescoWater treatmenteng
dc.subject.unescoQuímica del aguaspa
dc.subject.unescoWater chemistryeng
dc.titleTratamiento de un agua residual textil contaminada con colorante negro ácido 194 mediante un proceso Electro-Fentonspa
dc.title.translatedTreatment of textile wastewater contaminated with Acid Black 194 dye using an Electro-Fenton processeng
dc.typeTrabajo de grado - Maestríaspa
dc.type.coarhttp://purl.org/coar/resource_type/c_bdccspa
dc.type.coarversionhttp://purl.org/coar/version/c_ab4af688f83e57aaspa
dc.type.contentTextspa
dc.type.driverinfo:eu-repo/semantics/masterThesisspa
dc.type.versioninfo:eu-repo/semantics/acceptedVersionspa
dcterms.audience.professionaldevelopmentBibliotecariosspa
dcterms.audience.professionaldevelopmentEstudiantesspa
dcterms.audience.professionaldevelopmentInvestigadoresspa
dcterms.audience.professionaldevelopmentMaestrosspa
dcterms.audience.professionaldevelopmentMedios de comunicaciónspa
dcterms.audience.professionaldevelopmentPúblico generalspa
oaire.accessrightshttp://purl.org/coar/access_right/c_abf2spa
oaire.awardtitleTecnologías alternativas para el tratamiento de aguas residuales de la industria textil, Convocatoria de Proyectos Conectando Conocimiento (Convocatoria 852–2019, Proyecto: 202010034716, Contrato: 172–2021, HERMES-46681)spa
oaire.awardtitleConvocatoria para el Fortalecimiento de la Investigación, Creación, e Innovación articulado con la Formación en la Universidad Nacional de Colombia 2020–2021 (Proyectos: HERMES-51167 y HERMES-51225)spa
oaire.fundernameMinCienciasspa
oaire.fundernameUniversidad Nacional de Colombiaspa

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