Obtención y caracterización de películas nanoestructuradas de austenita expandida depositadas sobre acero inoxidable empleando la técnica de pulverización catódica magnetrón cc en fase reactiva
| dc.contributor.advisor | Garzón Ospina, Carlos Mario | spa |
| dc.contributor.author | Vergara Lozano, Giovanny Andrés | spa |
| dc.contributor.researchgroup | Microscopía eléctrónica | spa |
| dc.date.accessioned | 2020-07-02T20:32:20Z | spa |
| dc.date.available | 2020-07-02T20:32:20Z | spa |
| dc.date.issued | 2019 | spa |
| dc.description.abstract | Por medio de pulverización catódica en atmósfera reactiva se depositaron películas nanoestructuradas, cristalinas y sin nitruros de cromo, sobre sustratos de acero utilizando un blanco del acero austenítico UNS S31603. Estas presentaron estructura ferrítica, austenítica, dúplex (ferrita + austenita) o nitruro MN (M: metal), dependiendo de los parámetros de operación del reactor y del flujo de N2. La concentración de nitrógeno varió desde cero (Ar 1,2 sccm) hasta cerca de 50 %-at (Ar 1,2 sccm + N2 11,2 sccm). La dureza de las películas estuvo entre 8 – 13 GPa, mientras la dureza del blanco fue 2 – 3 GPa. El carácter dúctil – frágil de las películas varió, desde ductilidad muy elevada hasta comportamiento frágil ante cargas de indentación. De forma similar, se obtuvieron películas con elevada adherencia y baja cohesión al sustrato. Este trabajo propone un análisis para explicar la dependencia entre los parámetros de operación del reactor, la estructura, las propiedades mecánicas y las adherencias observadas. | spa |
| dc.description.abstract | Stainless Steel (SS) crystalline films, with no chromium nitride formation, were deposited on SS substrates by reactive sputtering, using a UNS S31603 target. Films obtained showed different structures, namely ferrite, austenite, duplex (ferrite + austenite) and MN nitride, according to both operational reactor parameters and N2 flow rate. Nitrogen uptake in film varied between N-lean films (Ar 1,2 sccm) up to near 50 %-at N (Ar 1,2 sccm + N2 11,2 sccm). Films hardness varied 8-13 GPa, while target hardness was around 2 – 3 GPa. Film ductile vs fragile character varied from very high ductile films, up to films with fragile performance films under contact indentation loads. In a similar manner, film-substrate adherence varied from extremely high up to films with cohesive failure, in both micro-indentation and scratch test. In this research, a depth analysis of sputtering parameters, film structure, and film tribomechanical performance is presented. | spa |
| dc.description.degreelevel | Maestría | spa |
| dc.format.extent | 137 | spa |
| dc.format.mimetype | application/pdf | spa |
| dc.identifier.uri | https://repositorio.unal.edu.co/handle/unal/77731 | |
| dc.language.iso | spa | spa |
| dc.publisher.branch | Universidad Nacional de Colombia - Sede Bogotá | spa |
| dc.publisher.program | Bogotá - Ingeniería - Maestría en Ingeniería - Materiales y Procesos | spa |
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| dc.rights | Derechos reservados - Universidad Nacional de Colombia | spa |
| dc.rights.accessrights | info:eu-repo/semantics/openAccess | spa |
| dc.rights.license | Atribución-NoComercial-SinDerivadas 4.0 Internacional | spa |
| dc.rights.spa | Acceso abierto | spa |
| dc.rights.uri | http://creativecommons.org/licenses/by-nc-nd/4.0/ | spa |
| dc.subject.ddc | 660 - Ingeniería química::669 - Metalurgia | spa |
| dc.subject.ddc | 620 - Ingeniería y operaciones afines::629 - Otras ramas de la ingeniería | spa |
| dc.subject.proposal | adherence | eng |
| dc.subject.proposal | adherencia | spa |
| dc.subject.proposal | MN nitride | eng |
| dc.subject.proposal | ensayo de rayado | spa |
| dc.subject.proposal | nitrógeno en aceros | spa |
| dc.subject.proposal | Nano hardness | eng |
| dc.subject.proposal | nitruro MN | spa |
| dc.subject.proposal | nitrogen in steels | eng |
| dc.subject.proposal | scratch test | eng |
| dc.subject.proposal | película de acero inoxidable | spa |
| dc.subject.proposal | pulverización catódica reactiva | spa |
| dc.subject.proposal | stainless steel film | eng |
| dc.subject.proposal | reactive sputtering | eng |
| dc.subject.proposal | nanodureza | spa |
| dc.title | Obtención y caracterización de películas nanoestructuradas de austenita expandida depositadas sobre acero inoxidable empleando la técnica de pulverización catódica magnetrón cc en fase reactiva | spa |
| dc.type | Trabajo de grado - Maestría | spa |
| dc.type.coar | http://purl.org/coar/resource_type/c_bdcc | spa |
| dc.type.coarversion | http://purl.org/coar/version/c_970fb48d4fbd8a85 | spa |
| dc.type.content | Text | spa |
| dc.type.driver | info:eu-repo/semantics/masterThesis | spa |
| dc.type.version | info:eu-repo/semantics/publishedVersion | spa |
| oaire.accessrights | http://purl.org/coar/access_right/c_abf2 | spa |